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Quality Requirements Edition 6.0                                                                                  European Enamel Association




            8.6      Testing of porcelain and vitreous enamel coatings                  29. to 33. day      daily water-replacement               (5  week)
                                                                                                                                                   th
                                                                                        34. and 35. day     no water-replacement
            8.6.1    Determination of resistance to boiling water by long-term exposure   36. to 40. day    daily water-replacement               (6  week)
                                                                                                                                                   th
                                                                                        41. and 42. day     day no water-replacement
            Purpose and scope
                                                                                        43. day             The test plates are, cleaned, dried and weighed.
            The vitreous enamel coating of devices and receptacles, that have to face repetition
            of stress by means of boiling or hot water, is tested for its resistance by a long-term   Testing-device
            exposure. Because of the high expenditure of time that is necessary for the test  -
                                                                                       Apparatus according to EN ISO 28706-2/6
            especially for hot water tanks - a suitable testing method must be followed.
                                                                                       Testing-time

            Method of testing                                                          If no further arrangements have been made, a testing-time of 2 x 3 weeks is valid; the
            The tests will be made according to EN ISO 28706-2 and the DIN 4753. The testing   second testing round is rated.
            time is set for 6 weeks. The tested plate is installed at the bottom of the apparatus
            while the top plate (vapour phase) is a glass-plate (borosilicate glass 3.3 according   Testing-temperature
            to DIN ISO 3585). The test solution is demineralised water with a conductivity of max.   If no further arrangements have been made, the test is realised at boiling temperature
            1 μS/cm and renewed according to the following scheme:                     using a condenser and graduated collector such as described in EN ISO 28706-2/6 and
                                                                                       following procedure EN ISO 28706-2/8 for its usage.
              1. to 5. day      daily water-replacement               (1  week)
                                                                       st

              6. and 7. day     no water-replacement                                   Test plates
              8. to 12. day     daily water-replacement               (2  week)
                                                                       nd
              13. and 14. day   no water-replacement                                   The test plates should be made out of the same steel as the to be tested receptacle.
              15. to 19. day    daily water-replacement               (3  week)        Because of the weighing accuracy, the plates should not be thicker than 2 mm. The
                                                                       rd
              20. and 21. day   no water-replacement                                   enamelling should be of a thickness of at least 0.25 mm and its surface should be free
                                                                       th
              22. day           The test plates are removed out of the   (4  week)     of weak or defective spots.
                                device and are cleaned and weighed.
                                After the weighing, the test plates are put            The test plates can be produced either in the laboratory or in the enamel shop. In the
                                in the device again.                                   last case, the test plates should be hooked on a stainless-steel hook and should be
                                The second testing round starts just like              fired in the interior of a receptacle of the production. Using this method, the sample
                                the first day                                          enamelling gains the same thermal treatment experience as the receptacle-enamelling.
              23. to 26. day    daily water-replacement               (4  week tbc)    Three test plates have to be tested. The average weight loss should not be higher than
                                                                       th
                                                                                            2
              27. and 28. day   no water-replacement                                   12 g/m .

            © EEA2025                                                                                                                                 page 118
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