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Quality Requirements Edition 6.0                                                                                  European Enamel Association




            8.5.4.2  Determination of the density of slips                             8.5.4.3  Determination of the flow behaviour of enamel slips by simple methods

            Purpose and scope                                                          Purpose and scope

            The density or specific gravity is the weight of one Liter of slip in kilogram. The slip   The meaning of this specification sheet is to determine the slip properties by simple
            density results from densities of the single components. Frit, quartz and clay have in   methods. The equipment required is reasonably priced and easy to handle, though
            average a density of 2.6 g/cm . There are also enamels available with a higher or   always the sum of several flow parameters is registered.
                                      3
            lower density. The frit supplier has this information. Water has a density of 1.0 g/ml.
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            Colouring oxides have very different densities. They can be as high as 4 g/cm  and   With the described equipment, the following is obtained:
            more. The small quantities of setting agents can be neglected by the calculation of
            the density of slips.                                                      1.  Dipping test sheet or cylinder Yield point and Thixotropy
                                                                                       2.  Enamel slip gauge       Viscosity and Thixotropy
            To  predetermine  the  slip  density,  divide  the  sum  of  the  weights  of  the  single   3.  Slump test   Viscosity and Thixotropy
            components by the sum of their volume.                                     4.  Outflow cup             Flow in pipes

            The fineness of grinding of the slip has no influence upon its density.    1. Dipping test and dipping cylinder
                                                                                       The flow of a slip can be simulated with plane or shaped sheet sections. By weighing
            Method of operation                                                        and conversion into one square meter of surface, the amount of slip left on the to be
                                                                                       enamelled  part  is  obtained.  This  amount  permits  an  estimation  of  the  subsequent
            One Liter or a part of the slip can be weight out. Normally, the PEMCO density meter
                                                                                       application thickness of enamel. This test method is among other things affected by
            with a volume of 100 ml is used.
                                                                                       varied manual draw-out velocities.

                                                                                       Method of operation:

                                                                                       A degreased test sheet of defined dimensions is dipped into the slip and withdrawn
                                                                                       obliquely.  After  the  excess  slip  has  drained  off,  the  amount  left  on  the  sheet  is
                                                                                       determined by weighing. Since the area of the sheet is readily measured, it is easy to
                                                                                       calculate the specific amount applied.

                                                                                       There is no need for any calculation if the same sheet is used frequently. Then the applied
                                                                                       weight is a direct measure. For external use, the application weight has to be expressed in
                                                                                       g/m , because the size of the test sheet is unknown to the interlocutor. In order to fit a
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            © EEA2025                                                                                                                                 page 115
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