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Quality Requirements Edition 5.0                                                                                  European Enamel Association






            4.10 Determination  of the adherence of the porcelain and vitreous enamel to the   100 grams sodium pyrophosphate (analytical grade)
            substrate                                                                     1000 ml distilled water
                                                                                       The solution should be freshly prepared.
            The testing of the adherence of the porcelain and vitreous enamel coating should be
            carried out using the method as specified in EN10209 Annex C.              The  test  should  be  carried  out  for  5 hours  of hard  boiling  during  which  heavy  vapour

                                                                                       bubbles must be rising from the bottom of the apparatus. The effect is measured by the loss
            4.11 Determination of the resistance to thermal shock
                                                                                                                          2
                                                                                       of mass of the test plates and given in g/m . (This test solution will need to be made up
            The  determination  of the  resistance  to thermal  shock  should  be  carried  out  using  the
                                                                                       hot as the solubility at 20º C is approximately 50 g/L, and also that this test solution is twice
            methods as specified in ISO 2747, unless the objects concerned are not suitable for this   the concentration of that used in the ”Hoover” test.)
            test method.  In these  cases  the test method  should  be agreed  and specified  in the

            quality requirements.                                                      4.16 Determination of the permeability to hydrogen

                                                                                       The determination of the permeability of a steel to hydrogen should be carried out using the
            4.12 Determination of the porosity by the high voltage test (destructive)     methods as specified in EN 10209 Annex A1.
            The determination of the porosity by the high voltage test of the porcelain and vitreous
                                                                                       See part 3.3 of EN 14866/December 2003.
            enamel coating should be carried out using the methods as specified in ISO 2746 and EN

            ISO 28721-1/4.3. High voltage test at 20 kV – subsequently 12 kV           4.17 Determination of gloss
                                                                                         The determination of gloss should be carried out using the methods as specified in EN ISO
            4.13 Determination, detection and location of defects (non-destructive)
                                                                                       2813. (This covers measurements at 20º, 60º and 85º. The USA measure specular gloss
            The non-destructive determination and detection of defects in the porcelain and vitreous
                                                                                       of ceramic surfaces at 45º {ASTM C246} – The angle of measurement must be specified
            enamel coating should be carried out using either method A or B as specified in EN ISO
            8289-1. The test method selected should depend on the specific application circumstances   by agreement.)
            EN ISO 8289-2 will apply for enamel slurry.
                                                                                       4.18 Determination of scratch resistance
                                                                                       The determination of scratch resistance should be carried out using the methods as
            4.14 Determination of the resistance to abrasion                           specified in EN ISO in
            Now see 4.26                                                               15695.


            4.15 Determination of the resistance to chemical corrosion by boiling of a solution   4.19 Determination of colour difference
            of sodium pyrophosphate                                                    The determination of colour difference should be carried out using the methods as

            The definition of the resistance to chemical corrosion of a solution of sodium    specified in ISO 11664and ISO 18314.
            pyrophosphate should be carried out using EN ISO 28706-2/15 (see 4.7), using the
            following test solution:                                                     4.20 Determination of edge coverage

                                                                                       The determination of edge coverage should be carried out using the method as specified
                                                                                       in EN ISO 28723.
            © EEA2020                                                                                                                                 page 19
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