Page 109 - 20250602 EEA QM Edition 6.0
P. 109

Quality Requirements Edition 6.0                                                                                  European Enamel Association




            Required reagents:
                                                                                       8.5.1   Testing of setting agents and other accessory materials
            Methylene blue solution (I)

                Dissolve 3.2 mg methylene blue in 500 ml distilled water of about 70  C. Put   Purpose and scope
                                                                           0
                this solution in a 1000 ml measuring flask and fill up at 20  C with distilled
                                                                    0
                                                                                       Testing of setting agents and other accessory materials can mostly be done in  the
                water.
                                                                                       laboratory  of  the  enamelling  shop.  The  various  analytical  processes  presuppose

                                                                                       training and experience.
            Methylene blue solution (II)
                                                                        0
                Dissolve 1.6 g methylene blue in 500 ml distilled water of about 70  C. Put this   Normally, setting agents are genuine or chemically pure chemicals supplied by the
                                                             0
                solution in a 1000 ml measuring flask and fill up at 20  C with distilled water.   chemical industry with their final quality control.

            6n sulphuric acid                                                          It is substantial for the processing plant to store the setting agents according to their
                                                                                       storage specifications. Some of them, e.g. sodium aluminate, are hygroscopic. That is
                Mix 167 ml concentrated H2SO4 (Density 1.84) with 700 ml distilled water and
                fill up to 1000 ml with distilled water.                               to say, they adsorb water, so that the agent cannot be used for enamelling if not stored
                                                                                       properly.



                                                                                       In  case  of  doubt  about  the  correct  storage  of  accessory  materials,  suppliers  or
                                                                                       manufacturers should be contacted for the corresponding specifications.

















            © EEA2025                                                                                                                                 page 109
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